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Fabrication of yttria-doped zirconia-alumina composite ceramics with high strength and fracture toughness by pulsed electric-current pressure sintering
https://doi.org/10.14988/pa.2017.0000014266
https://doi.org/10.14988/pa.2017.0000014266032b6375-8334-4986-88aa-e9d993985b77
名前 / ファイル | ライセンス | アクション |
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023056030001.pdf (18.7 MB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||||||||||||||
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公開日 | 2015-12-03 | |||||||||||||||||
タイトル | ||||||||||||||||||
言語 | en | |||||||||||||||||
タイトル | Fabrication of yttria-doped zirconia-alumina composite ceramics with high strength and fracture toughness by pulsed electric-current pressure sintering | |||||||||||||||||
言語 | ||||||||||||||||||
言語 | eng | |||||||||||||||||
キーワード | ||||||||||||||||||
主題 | 酸化ジルコニウム(ZrO2), 酸化アルミニウム(Al2O3), 固溶体, 中和共沈法, パルス通電加圧焼結 (PECPS) Zirconium oxide (ZrO2), aluminum oxide (Al2O3), neutralization co-precipitation method, pulsed electric-current pressure sintering (PECPS), solid solution |
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資源タイプ | ||||||||||||||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||||||||||||||
資源タイプ | departmental bulletin paper | |||||||||||||||||
ID登録 | ||||||||||||||||||
ID登録 | 10.14988/pa.2017.0000014266 | |||||||||||||||||
ID登録タイプ | JaLC | |||||||||||||||||
アクセス権 | ||||||||||||||||||
アクセス権 | open access | |||||||||||||||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||||||||||||||
その他(別言語等)のタイトル | ||||||||||||||||||
その他のタイトル | パルス通電加圧焼結を用いたイットリア添加ジルコニア-アルミナコンポジットセラッミクの作製 | |||||||||||||||||
言語 | ja | |||||||||||||||||
その他(別言語等)のタイトル | ||||||||||||||||||
その他のタイトル | パルス ツウデン カアツ ショウケツ オ モチイタ イットリア テンカ ジルコニア-アルミナ コンポジット セラッミク ノ サクセイ | |||||||||||||||||
言語 | ja-Kana | |||||||||||||||||
著者 |
廣田, 健
× 廣田, 健
WEKO
15901
× 山本, 健太× 笹井, 厚希× 加藤, 将樹
WEKO
15903
× 田口, 秀樹× 木村, 英夫× 高井, 優行× 寺田, 昌生 |
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著者所属(英) | ||||||||||||||||||
en | ||||||||||||||||||
Hirota, Ken / 同志社大学理工学部機能分子・生命化学科教授 | ||||||||||||||||||
著者所属(英) | ||||||||||||||||||
en | ||||||||||||||||||
Kato, Masaki / 同志社大学理工学部機能分子・生命化学科教授 | ||||||||||||||||||
著者所属(英) | ||||||||||||||||||
en | ||||||||||||||||||
Taguchi, Hideki / Graduate School of Natural Science and Technology, Okayama University | ||||||||||||||||||
著者所属(英) | ||||||||||||||||||
en | ||||||||||||||||||
Terada, Masao / Daiichi Kigenso Kagaku Kogyo Co., Ltd. | ||||||||||||||||||
抄録 | ||||||||||||||||||
内容記述タイプ | Abstract | |||||||||||||||||
内容記述 | 中和共沈法で調製した立方晶ZrO[2] 固溶体のナノ粒子粉体をAr中1598 K、 600 s、圧力50~60 MPaの条件でパルス通電加圧焼結(PECPS)して、10~30mol%のAl[2]O[3]と1.5 mol%のY[2]O[3]を含んだZrO[2]-Al[2]O[3]コンポジットセラミックス、即ち90~70mol% ZrO[2] (1.5mol% Y[2]O[3])-10~30mol% Al[2]O[3]組成のセラミックスを作製した。 Y[2]O[3]を添加した正方晶ZrO[2] ([ss])とα-Al[2]O[3]から構成された緻密なコンポジットセラミックスは、粒子径280~130 nmの結晶粒子から構成されていた。FE-SEMによる観察からその微細構造、即ち、正方晶ZrO[2]とα-Al[2]O[3]の結晶粒径、およびα-Al[2]O[3]粒子の分布は、α-Al[2]O[3]の含有量に大きく依存することが分かった。Al[2]O[3]含有量が最適組成の25mol%、相対密度が99.9%のコンポジットセラミックスで、極端に高い機械的特性である曲げ強度(σ[b]≥1 GPa)と強靱性([K][IC]≥15 MPa·m[1/2])が同時に達成された。この組成は熱間静水圧プレスで作製されたZrO[2](2~3mol%Y[2]O[3])-Al[2]O[3]セラミックスと同じ組成であった。 | |||||||||||||||||
言語 | ja | |||||||||||||||||
抄録 | ||||||||||||||||||
内容記述タイプ | Abstract | |||||||||||||||||
内容記述 | ZrO[2]-Al[2]O[3] composite ceramics containing 10~30 mol% Al[2]O[3] and 1.5 mol% Y[2]O[3], [i.e.], 90~70 mol% ZrO[2] (1.5 mol% Y[2]O[3])-10~30 mol% Al[2]O[3] ceramics, have been fabricated by pulsed electric-current pressure sintering (PECPS) of cubic ZrO[2] solid solution([ss]) nano-powders prepared via the neutralization co-precipitation method, at 1598 K for 600 s under 50~60 MPa in Ar. Y[2]O[3]-doped tetragonal-ZrO[2] ([ss])/α-Al[2]O[3] dense ceramics were composed of 280-130 nm grains. FE-SEM observation revealed that their microstructures, that is the grain sizes of both t-ZrO[2]([ss]) and α-Al[2]O[3], and the distribution of α-Al[2]O[3] grains, were much influenced by the content of α-Al[2]O[3]. The best mechanical properties of extreme high bending strength (σ[b] ≥ 1 GPa) and high fracture toughness ([K][IC] ≥ 15 MPa·m[1/2]) were attained simultaneously at the composition of 25 mol% Al[2]O[3] with a high relative density of 99.9%, as the same composition reported on the hot isostatic press (HIP) sintered ZrO[2] (2~3 mol%Y[2]O[3])-Al[2]O[3] composite ceramics. | |||||||||||||||||
言語 | en | |||||||||||||||||
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内容記述タイプ | Other | |||||||||||||||||
内容記述 | 抄録中の[i.e.][ss][K]は斜体文字、[1/2]は上付き文字、[2][3][IC][b]は下付き文字 | |||||||||||||||||
言語 | ja | |||||||||||||||||
書誌情報 |
ja : 同志社大学ハリス理化学研究報告 en : The Harris science review of Doshisha University 巻 56, 号 3, p. 133-139, 発行日 2015-10-31 |
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言語 | ja | |||||||||||||||||
出版者 | 同志社大学ハリス理化学研究所 | |||||||||||||||||
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言語 | en | |||||||||||||||||
出版者 | Harris Science Research Institute of Doshisha University | |||||||||||||||||
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収録物識別子タイプ | PISSN | |||||||||||||||||
収録物識別子 | 21895937 | |||||||||||||||||
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収録物識別子タイプ | NCID | |||||||||||||||||
収録物識別子 | AA12716107 | |||||||||||||||||
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権利者名 | 同志社大学ハリス理化学研究所 | |||||||||||||||||
言語 | ja | |||||||||||||||||
権利者名 | Harris Science Research Institute of Doshisha University | |||||||||||||||||
言語 | en | |||||||||||||||||
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関連タイプ | isFormatOf | |||||||||||||||||
識別子タイプ | URI | |||||||||||||||||
関連識別子 | https://doors.doshisha.ac.jp/opac/opac_link/bibid/SB12902196/?lang=0 | |||||||||||||||||
言語 | ja | |||||||||||||||||
関連名称 | 掲載刊行物所蔵情報へのリンク / Link to Contents | |||||||||||||||||
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内容記述タイプ | Other | |||||||||||||||||
内容記述 | application/pdf | |||||||||||||||||
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出版タイプ | VoR | |||||||||||||||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||||||||||||||
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主題 | 501.49 |