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Metal compound analysis by capillary chromatography using an untreated capillary tube and water-hydrophilic-hydrophobic solvent mixture as a carrier solution
https://doi.org/10.14988/pa.2017.0000012309
https://doi.org/10.14988/pa.2017.0000012309c580b805-c0ea-4518-a799-c48f4083b792
名前 / ファイル | ライセンス | アクション |
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023051040002.pdf (143.2 kB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2011-03-09 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Metal compound analysis by capillary chromatography using an untreated capillary tube and water-hydrophilic-hydrophobic solvent mixture as a carrier solution | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題 | Capillary chromatography, Laminar flow conditions, Tube radial distribution, Chemiluminescence detection, Metal compound | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
ID登録 | ||||||
ID登録 | 10.14988/pa.2017.0000012309 | |||||
ID登録タイプ | JaLC | |||||
アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
著者 |
Yoshida, Kazuma
× Yoshida, Kazuma× Jinno, Naoya× Hashimoto, Masahiko× Tsukagoshi, Kazuhiko |
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著者所属(英) | ||||||
en | ||||||
Tsukagoshi, Kazuhiko / Department of Chemical Engineering and Materials Science, Faculty of Science and Engineering, Doshisha University | ||||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | 管径方向分配クロマトグラフィー(TRDC)システムは未修飾のオープンキャピラリーチューブと水-親水性/疎水性有機溶媒混合液をキャリア溶液として用いる。我々は化学発光検出器を備えたTRDCシステムにより硫酸銅、ヘマチン、ヘモグロビンのような金属化合物を分析した。モデル試料のヘマチンと銅(II)イオンおよびヘモグロビンと銅(II)イオンの混合液を落差法によってフューズドシリカキャピラリー内に注入した後に、水-アセトニトリル-酢酸エチルを体積比2:7:4および15:2:1で混合したキャリア溶液をマイクロシリンジポンプを用いて送液した。ヘマチンと銅(II)イオンおよびヘモグロビンと銅(II)イオンは有機溶媒過剰のキャリア溶液を用いた場合には管径方向への分配に基づき良好に分離して順に溶出し、化学発光により検出された。 | |||||
言語 | ja | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A tube radial distribution chromatography (TRDC) system was developed using an untreated open capillary tube and a water-hydrophilic-hydrophobic solvent mixture as a carrier solution. We examined metal compounds such as copper(II) sulfate, hematin, and hemoglobin using the TRDC system equipped with chemiluminescence detector. The model mixture solutions of hematin–copper(II), and hemoglobin– copper(II), were injected into a fused-silica capillary tube by the gravity method and subsequently delivered with the carrier solutions of water–acetonitrile–ethyl acetate (2:7:4 volume ratio) and water–acetonitrile–ethyl acetate (15:2:1 volume ratio), respectively, using a microsyringe pump. The mixture of hematin–copper(II) as well as hemoglobin–copper(II) was well separated and eluted with the organic solvent-rich carrier solution based on the tube radial distribution and detected by chemiluminescence in the present TRDC system. | |||||
言語 | en | |||||
書誌情報 |
ja : 同志社大学理工学研究報告 en : The Science and Engineering Review of Doshisha University 巻 51, 号 4, p. 8-11, 発行日 2011-01-31 |
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出版者 | ||||||
言語 | ja | |||||
出版者 | 同志社大学理工学研究所 | |||||
出版者(英) | ||||||
言語 | en | |||||
出版者 | Science and Engineering Research Institute of Doshisha University | |||||
ISSN | ||||||
収録物識別子タイプ | PISSN | |||||
収録物識別子 | 00368172 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN00165868 | |||||
権利者情報 | ||||||
権利者名 | 同志社大学理工学研究所 | |||||
言語 | ja | |||||
権利者名 | Science and Engineering Research Institute of Doshisha University | |||||
言語 | en | |||||
関連サイト | ||||||
関連タイプ | isFormatOf | |||||
識別子タイプ | URI | |||||
関連識別子 | https://doors.doshisha.ac.jp/opac/opac_link/bibid/SB00960326/?lang=0 | |||||
言語 | ja | |||||
関連名称 | 掲載刊行物所蔵情報へのリンク / Link to Contents | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
出版タイプ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
日本十進分類法 | ||||||
主題 | 433.45 |