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Temperature effect on separation performance in capillary chromatography based on tube radial distribution of aqueous-organic mixture carrier solvents
https://doi.org/10.14988/pa.2017.0000012262
https://doi.org/10.14988/pa.2017.0000012262d58ec49e-c773-47a9-bbad-6f877d828714
名前 / ファイル | ライセンス | アクション |
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023051030005.pdf (125.1 kB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2010-11-30 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Temperature effect on separation performance in capillary chromatography based on tube radial distribution of aqueous-organic mixture carrier solvents | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題 | Capillary chromatography, Laminar flow conditions, Tube radical distribution, Capillary temperature, The van't Hoff equation | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
ID登録 | ||||||
ID登録 | 10.14988/pa.2017.0000012262 | |||||
ID登録タイプ | JaLC | |||||
アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
著者 |
Jinno, Naoya
× Jinno, Naoya× Hashimoto, Masahiko× Tsukagoshi, Kazuhiko |
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著者所属(英) | ||||||
en | ||||||
Jinno, Naoya / Department of Chemical Engineering and Materials Science, Faculty of Science and Engineering, Doshisha University | ||||||
著者所属(英) | ||||||
en | ||||||
Hashimoto, Masahiko / Department of Chemical Engineering and Materials Science, Faculty of Science and Engineering, Doshisha University | ||||||
著者所属(英) | ||||||
en | ||||||
Tsukagoshi, Kazuhiko / Department of Chemical Engineering and Materials Science, Faculty of Science and Engineering, Doshisha University | ||||||
所属機関識別子種別 | ||||||
値 | kakenhi | |||||
所属機関識別子 | ||||||
値 | 34310 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | 我々は,フューズドシリカ,ポリエチレン,またはポリテトラフルオロエチレン製のオープンキャピラリーと水-親水性-疎水性有機溶媒混合キャリア溶液を用いたキャピラリークロマトグラフィーを開発した.この管径方向分配クロマトグラフィー(TRDC)システムは,層流条件下で実行される.これまでに,フューズドシリカキャピラリーと水-アセトニトリル-酢酸エチル混合キャリア溶液を用いて,TRDCシステムにおける分離挙動の温度の影響について調べた.モデル試料中の1-ナフトールと2,6-ナフタレンジスルホン酸は,有機溶媒過剰キャリア溶液を用いて温度範囲5-23℃でベースライン分離して溶出した.この研究では,キャリア溶液の管径方向分配に基づいたキャピラリーチューブ内でのinner相とouter相の形成が一定であるという仮定のもと,様々なキャピラリー温度で得られたクロマトグラムにvan't Hoffの式を適用することを試みた. | |||||
言語 | ja | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | We have developed a capillary chromatography system using an open capillary tube made of fused-silica, polyethylene, or poly(tetrafluoroethylene), and a water-hydrophilic/hydrophobic organic mixture carrier solution. This so-called tube radial distribution chromatography (TRDC) system works under laminar flow conditions. Previously, the effects of capillary temperature on separation performance in the TRDC system were examined using a fused-silica capillary tube and a water-acetonitrile-ethyl acetate mixture carrier solution; 1-naphthol and 2,6-naphthalenedisulfonic acid in a model mixture were eluted with baseline separation over the temperature range of 5 – 23°C with the organic solvent-rich carrier solution. In this study, based on the assumption that the phase distribution of inner and outer phases in the capillary tube induced by the tube radial distribution of the carrier solvents did not change with temperature over a limited range, we attempted to apply the van't Hoff equation to the chromatographic data obtained at various capillary temperature. | |||||
言語 | en | |||||
書誌情報 |
ja : 同志社大学理工学研究報告 en : The Science and Engineering Review of Doshisha University 巻 51, 号 3, p. 32-36, 発行日 2010-10-31 |
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出版者 | ||||||
言語 | ja | |||||
出版者 | 同志社大学理工学研究所 | |||||
出版者(英) | ||||||
言語 | en | |||||
出版者 | Science and Engineering Research Institute of Doshisha University | |||||
ISSN | ||||||
収録物識別子タイプ | PISSN | |||||
収録物識別子 | 00368172 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN00165868 | |||||
権利者情報 | ||||||
権利者名 | 同志社大学理工学研究所 | |||||
言語 | ja | |||||
権利者名 | Science and Engineering Research Institute of Doshisha University | |||||
言語 | en | |||||
関連サイト | ||||||
関連タイプ | isFormatOf | |||||
識別子タイプ | URI | |||||
関連識別子 | https://doors.doshisha.ac.jp/opac/opac_link/bibid/SB00960326/?lang=0 | |||||
言語 | ja | |||||
関連名称 | 掲載刊行物所蔵情報へのリンク / Link to Contents | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
出版タイプ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
日本十進分類法 | ||||||
主題 | 433.4 |